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In the determination of silicon content in an organic sample, a small and accurately-measured quantity of a substance is added to the large amount of sulfuric acid, then heated in an evaporating dish. The dish is heated with a Bunsen burner, until only stable precipitate remains, which contains the silica content. The dish is then closed and heated at high temperature until completely clean, fused silica is produced. Comparison of the initial weight of the substance and that of the fused silica allows the content of silicon in the sample to be determined.